Friction extrusion processing of aluminum powders: Microstructure homogeneity and mechanical properties

Friction extrusion processing of aluminum powders: Microstructure homogeneity and mechanical properties

CHAN Chang Yin-Cheng, RATH Lars, SUHUDDIN Uceu F. H., KLUSEMANN Benjamin

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Abstract. Friction extrusion (FE) is a solid-state process categorized as an energy-efficient process, utilizing the intrinsic friction-induced heat to plasticize and manufacture fully consolidated extrudate from various feedstocks, i.e. solid billet, chips and powder. Friction in the relative motion between the feedstock and the non-consumable die generates heat as well as imposes severe plastic deformation; this combination enables dynamic recrystallization and refinement of the microstructure. This study demonstrates the feasibility of directly extruding aluminum alloy powder into fully consolidated wire in a single step process. The extrudate is free of noticeable defects and shows predominantly homogeneous microstructure along the cross-section of the wire. The powder evolution upon passing through the die orifice was investigated in terms of morphology and microstructure. Additionally, the mechanical properties of the extrudate, i.e. microhardness and ultimate tensile strength, were compared to solid billets of AA7075 in different temper states and shows adequate mechanical properties without possible post-heat treatments.

Keywords
Friction Extrusion, Solid-State Processing, Aluminum, Powder Consolidation

Published online 4/19/2023, 8 pages
Copyright © 2023 by the author(s)
Published under license by Materials Research Forum LLC., Millersville PA, USA

Citation: CHAN Chang Yin-Cheng, RATH Lars, SUHUDDIN Uceu F. H., KLUSEMANN Benjamin, Friction extrusion processing of aluminum powders: Microstructure homogeneity and mechanical properties, Materials Research Proceedings, Vol. 28, pp 515-522, 2023

DOI: https://doi.org/10.21741/9781644902479-56

The article was published as article 56 of the book Material Forming

Content from this work may be used under the terms of the Creative Commons Attribution 3.0 license. Any further distribution of this work must maintain attribution to the author(s) and the title of the work, journal citation and DOI.

References
[1] W.M. Thomas, E.D. Nicholas and S.B. Jones, U.S. Patent 5,262,123. (1993).
[2] W. Tang, A.P. Reynolds, Production of wire via friction extrusion of aluminum alloy machining chips, J. Mater. Process. Technol. 210 (2010) 2231-2237. https://doi.org/10.1016/j.jmatprotec.2010.08.010
[3] G. Buffa, D. Campanella, L. Fratini, F. Micari, AZ31 magnesium alloy recycling through friction stir extrusion process, Int. J. Mater. Form. 9 (2016) 613-618. https://doi.org/10.1007/s12289-015-1247-6
[4] X. Li, N. Overman, T. Roosendaal, M. Olszta, C. Zhou, H. Wnag, T. Perry, J. Schroth, G. Grant, Microstructure and Mechanical Properties of Pure Copper Wire Produced by Shear Assisted Processing and Extrusion, JOM 71 (2019) 4799-4805. https://doi.org/10.1007/s11837-019-03752-w
[5] M.A. Ansari, R.A. Behnagh, M. Narvan, E.S. Naeini, M.K.B. Givi, H. Ding, Optimization of Friction Stir Extrusion (FSE) Parameters Through Taguchi Technique, Trans. Indian Inst. Met. 69 (2016) 1351-1357.
[6] D. Baffari, A.P.Reynolds, X. Li, L. Fratini, Influence of processing parameters and initial temper on Friction Stir Extrusion of 2050 aluminum alloy, J. Manuf. Process. 28 (2017) 319-325. https://doi.org/10.1016/j.jmapro.2017.06.013
[7] J.T. Darsell, N.R. Overman, V.V. Joshi, S.A. Whalen, S.N. Mathaudhu, Shear Assisted Processing and Extrusion (ShAPE™) of AZ91E Flake: A Study of Tooling Features and Processing Effects, J. Mater. Eng. Perform. 27 (2018) 4150-4161. https://doi.org/10.1007/s11665-018-3509-1
[8] R.M. Halak, L. Rath, U.F.H.R. Suhuddin, J.F. dos Santos, B. Klusemann, Changes in processing characteristics and microstructural evolution during friction extrusion of aluminum, Int. J. Mater. Form. 15 (2022) 24. https://doi.org/10.1007/s12289-022-01670-y
[9] S. Whalen, M. Olszta, C. Roach, J. Darsell, D. Graff, M. Reza-E-Rabby, T. Roosendaal, W. Daye, T. Pelletiers, S. Mathaudhu, N. Overman, High ductility aluminum alloy made from powder by friction extrusion, Materialia 6 (2019) 100260. https://doi.org/10.1016/j.mtla.2019.100260
[10] X. Li, T. Wang, X. Ma, N. Overman, S. Whalen, D. Herling, K. Kappagantula, Manufacture aluminum alloy tube from powder with a single-step extrusion via ShAPE, J. Manuf. Process. 80 (2022) 108-115. https://doi.org/10.1016/j.jmapro.2022.05.060
[11] X. Li, C. Zhou, N. Overman, X. Ma, N. Canfield, K. Kappagantula, J. Schroth, G. Grant, Copper carbon composite wire with a uniform carbon dispersion made by friction extrusion, J. Manuf. Process. 65 (2021) 397-406. https://doi.org/10.1016/j.jmapro.2021.03.055
[12] M. Komarasamy, X. Li, S.A. Whalen, X. Ma, N. Canfield, M.J. Olszta, T. Varga, A.L. Schemer-Kohrn, A. Yu, N.R. Overman, S.N. Mathaudhu, G.J. Grant, Microstructural evolution in Cu–Nb processed via friction consolidation, J. Mater. Sci. 56 (2021) 12864-12880. https://doi.org/10.1007/s10853-021-06093-9
[13] X. Li, M. Reza-E-Rabby, A. Guzman, G. Grant, S. Mathaudhu, M. Hinton, A. Reynolds, Strain and strain rate in friction extrusion, J. Mater. Res. Technol. 22 (2022) 882-893. https://doi.org/10.1016/j.jmrt.2022.07.116
[14] G.B. Schaffer, S.H. Huo, On development of sintered 7xxx series aluminium alloys, Powder Metall. 42 (1999) 219-226. https://doi.org/10.1179/003258999665558
[15] D. Baffari, G. Buffa, D. Campanella, L. Fratini, A.P. Reynolds, Process mechanics in Friction Stir Extrusion of magnesium alloys chips through experiments and numerical simulation, J. Manuf. Process. 29 (2017) 41-49. https://doi.org/10.1016/j.jmapro.2017.07.010
[16] M.R. Rokni, C.A. Widener, G.A. Crawford, Microstructural evolution of 7075 Al gas atomized powder and high-pressure cold sprayed deposition, Surf. Coat. Technol. 251 (2014) 254-263. https://doi.org/10.1016/j.surfcoat.2014.04.035
[17] A. Hadrboletz, B. Weiss, Fatigue behaviour of iron based sintered material: a review, Int. Mater. Rev. 42 (1997) 1-44. https://doi.org/10.1179/imr.1997.42.1.1
[18] R. Kalsar, X. Ma, J. Darsell, D. Zhang, K. Kappagantula, D.R. Herling, V.V. Joshi, Microstructure evolution, enhanced aging kinetics, and mechanical properties of AA7075 alloy after friction extrusion, Mater. Sci. Eng. A. 823 (2022) 142575. https://doi.org/10.1016/j.msea.2021.142575